A. Lucas, 10/6/43: Notes on work done on some of the objects from the
tomb of Tutankhamun.
Meant for private use and reference only.
In addition, formal notes were made by me on many of the Index Cards
giving treatment of objects.
The importance of these notes is now such that we hope that Lucas would forgive us for making them public - Jaromir Malek.
Concept & Direction: Jaromir Malek
Scanning: Kent Rawlinson, Jenni Navratil
Transcription and editing: Lindsay Allen and Jaromir Malek
Coordination: Elizabeth Fleming
Season 1925-6
1
Luxor
Season 1925-26
A. Lucas
Second Coffin No 254
Body
Cleaned with warm water + NH4O4
Repaired with paraffin wax: painted with hot wax.
The body was inlaid like the lid + the dark blue glass was similarly badly deteriorated.
Lid
Eye
whites badly deteriorated on surface: impossible to be certain of what
compound, but probably CaCO3
Metal Tongues on Lid. Cleaned with ammonia + proved to be silver
Outermost Coffin No 253
Lid
Cleaned with warm water and NH4O4.
Repaired with celluloid cement.
Filled hollows in gesso with hot melted paraffin wax by means of a pipette
Painted with paraffin wax
Second Coffin No 254
Lid (Coloured cement under inlay)
Cleaned with warm water. (Face + hands with NH4O4)
Repaired in places with celluloid cement and in places with paraffin wax. Painted with hot wax.
G.R. 17/26
Thickness of some of the gold (a) 0.04 mm to 0.07mm.
(b) 0.03 mm to 0.07mm (c) 0.05 mm to 0.07 mm.
(c) 0.05 mm to 0.07 mm.
The lid was inlaid with coloured glass, two shades of blue - dark + light -
and red. The light blue and the red glass were both in excellent condition,
but the dark blue was badly deteriorated + in many instances had crumbled
+ swollen to a whitish powder. On analysis this powder gave no re-action
for Cl or SO3 but was alkaline + contained a carbonate (soluble)
and an insoluble residue.
G.R. 18/26
Several pieces of semi-transparent material with coloured design beneath
Repeated Ether Extraction + after evaporating off ether extracted fatty matter with xylol. Xylol extract (fatty matter) solid when cold.
3
Third Coffin. No 255
1/26 2/26
Black pitch-like material (? from libation)
Solvents
Acetone. Largely soluble. Solution dark brown + contained fatty matter; was
sticky when nearly dry (? resin) After removing fatty matter with xylol,
the residue was dry, brittle + resinous-looking.
Alcohol. Partly soluble. Solution dark brown.
Amyl Acetate. Very slight colour extracted.
Benzine. No colour extracted. (In spite of resemblance to wood pitch in smell the insolubility (except fatty matter) is against presence of wood pitch)
Ether. Very slight colour extracted: solution on evaporation left a liquid fatty matter, which was acid.
Xylol. No colour extracted: solution on evaporation left a liquid, white, fatty matter, which was acid
The black material was covered in parts with small white crystals suggestive of a fatty acid. This melted when hot.
The smell of the original material suggestive of wood pitch. The material burned with a smoky flame (melted + became resinous)
(The black material (? libation) on foot of outermost coffin No 253, appeared to be identical: it behaved the same with solvents but showed no white efflorescence)
255 The rose colour readily rubbed off
256 - do -
Gold Bands on Flail + Crook belonging to Hands 256
Various colours of red and also green: some of the red was KMnO4 coloured but the colours looked like interference films.
Organic Purple Colour
Sometimes a purplish stain on gold that appeared to be organic + can only
be removed by heating.
4
Gold - Colour of
Coffin 253 Generally very yellow: some discoloration on face.
Coffin 254 As for 253. Under side of Uraeus red (not rose)
Greyish-green powder on face.
Coffin 255 Very yellow. Vulture's head red (not rose): greyish-green
powder on foot + in places inside. Some gold beads of necklaces rose red.
Mask 256 Very yellow. Some gold beads of necklaces rose red.
Coffin 255 (Contd) In addition to vulture's head, the gold in other places on the upper part of figure, (but not at foot), as on beard + in patches on face + at side of breast, was very red (not rose)
Jewellery in coffin (RRR) Bib-like collarette on chest. Gold tubular
beads with granulated work: on some the gold outside except the granules was
rose, while in others it was very yellow: (insides not examined, except in
one case when the gold was rose)
Later 4 others were examined - these yellow inside.
Also in debris in coffin alongside the beads were a few gold sequins (small)
like those found on one of the robes. These yellow outside but all rose
inside.
Metal Pins fastening Lids to Coffins
253. Looked very like copper or bronze: and were very dark-coloured on the outside. On examination (after cleaning) proved to be of silver with gold beads soldered on. Both the gold + silver contains copper.
254 Like 253
255 Gold.
Cleaning
253. 254. 255 NH4OH + hot water.
6
Mask 256
Beard is of inlaid dark blue glass which has become light-greyish. Under
side gold.
Cleaned glass with warm water + gold with NH4OH + water
Face on Lid 255
Eyes badly deteriorated - whites look like some form of CaCO3:
pupils are obsidian: the whites came entirely to powder when touched.
A number of pieces of inlay were of semi-transparent material (that looked like glass) with a coloured cement (red) underneath. In one case where it was possible to examine this; it was not glass but a natural stone. It did not scratch with a knife blade and scratched glass + therefore was transparent quartz.
Mask 256
Collars (Three rows)
Practically identical with those on 255.
Cleaned in similar manner.
A few of the rose-coloured beads had patches of black resinous material.
This chipped off with a knife + finished cleaning in flame of spirit lamp.
Immediately on placing in water and also in acetone the red colour began to
become lighter + yellowish and to disappear but it seemed to darken again +
turn more red again on heating.
The dark blue glass inlay in one of the end pieces was badly deteriorated -
in some cases it had gone to a whitish powder + in other cases it retained
its shape but was white + friable: the light greenish-blue glass was in
good condition.
7
Coffin 255
Lid
H. Carter + H. Burton removed the greater part of the black material,
chiefly by mechanical means (chipping). Removed remainder with penknife and
afterwards with a rag soaked in acetone.
Cleaned gold with NH4OH.
On rebated edge in places there was a brown resin suggesting that this had
been used as a lute to help to fasten coffin + lid and to make the joint
airtight.
Washed with warm water + NH4OH.
(A piece of stick removes the reddish discolouration from the gold without
injury - stick wetted from time to time: this also cleans the surface of the
inlay)
Collars. (Two rows)
Composed of large flat disc-shaped beads of gold and faience. Some of the
gold beads were a rose-colour: these occurred at regular intervals in both
necklaces and there were always two rose-coloured beads together.
Cleaned: Rose-coloured beads with soft brush: faience with warm water
(dark-blue coloured faience of which a thin surface coating was peeling
off). Cleaned gold which was of a light grey colour suggesting silver with
NH4OH + warm water. In most cases came very yellow, but in a few
instances some discoloration remained: most of these latter came clean when
heated to dull red in a spirit lamp: in a few cases the colour became
darker (there seemed to be much copper in there) but with HlO3
followed by water, NH4OH + water again they came fairly yellow.
Ends were inlaid: thus cleaned with NH4OH + water
8
Flail No 255.
The handle of the flail was badly disintegrated, the covering material being broken off and the bronze (or copper) core being bare.
GR/5/26
The broken material was found to be glass which on the surface had lost its
original dark-blue colour and had become grey, though the interior was still
dark blue.
The breaking of the glass had possibly been due to the corrosion and
expansion of the metal core: the broken pieces were with few exceptions in
large pieces and were fairly solid, though there was some disintegration.
On some of the pieces of glass there were solidified globules of brown
resinous-looking material, almost certainly resin.
Cleaned flail with NH4OH + warm water.
Some of the threaded, truncated cone shaped stones were carnelian, some
were of turquoise-blue glass in good condition + some were almost in
powder + had probably been dark blue glass. Repaired one with celluloid
cement.
A small aggregate of crystals from inside coffin at upper end also consisted of NaCl.
G.R. 19/26
9
Mummy 256
Inside of abdomen packed with resinous material + doubled up fabric making the whole a hard, solid mass.
Flesh blackened and very brittle.
Bones blackened.
Bandages for most part blackened and powdery: in some few instances brown (dark) + fragile.
G.R. 19/26
Outside of skin from top of shoulders showed whitish spots looking very
like an eruption.
The whitish material was crystalline + consisted largely of NaCl but
contained some Na3SO4
GR 20/26
4 Q. Specimen of material from underneath diadem on head attaching vulture's head to serpent's head. This was brown + somewhat resembled beeswax (ancient + dry) in places but proved to be resin. It was slightly resinous looking in places, melted with heat, did not give a greasy stain on paper, insoluble in benzine but soluble in alcohol. No inorganic matter present (i.e. no admixture of whiting)
GR 21/26
From just below the nostrils (? plug). Black, porous material of light weight. This proved to be decayed woven fabric held together by a little resin
GR 22/26
Tiny specks of reddish material from right eye. With a lens this looked
very resinous: it was too small for a complete examination but was probably
resin.
Apparently only partly soluble in acetone + in alcohol.
Circlets JJ (from Mummy)
(a) 2 Blue glass + gold
(b) 2 Gold + inlay.
Gold cleaned with NH4OH + warm water
Glass inlay cleaned with warm water.
Dipped in hot melted paraffin wax (H.C.)
Circlets U. V. and W
(c) U was a duplicate of one of the JJ group
(d) V " " " " another " " " "
(e) W was glass + carnelian + gold
All cleaned as for JJ.
Circlet cc
(f) Duplicate of W. (glass, carnelian + gold)
In all 4 pairs
In several cases a little paraffin wax (from waxing beadwork adjoining) was removed with petroleum spirit.
A little fatty matter in some cases was removed with acetone
Repaired where necessary (i.e. b.c.d + f) by H.C. with glue + afterwards dipped in melted paraffin wax.
11
Finger Rings
ff (5 rings)
1 Green chalcedony
1 Lapis lazuli
1 Chalcedony scarab in gold mount.
1 Gold mount, lapis scarab, inlay (Repaired by HC with glue + waxed)
1 Gold with inlaid uraei - thin + poor (Dipped in melted paraffin wax)
Grease removed with acetone
Cleaned with warm water + gold with warm water + ammonia
VV (8 rings)
1 Resin
2 Solid gold
1 Gold foil on ? wood
1 Black resin
4 Scarabs in gold mounts
1 Turquoise with dark brownish red patches
1 Lapis lazuli
(a) 1 Quartz - slight green tint
x 1 Lapis (see below)
Resin cleaned with warm water only
Gold cleaned with warm water + ammonia
x Lapis now in 5 pieces (originally in 3) + is hollow (i.e. a shell) + is
filled with a whitish material which has expanded + split the lapis: gold
pins fixed in with a reddish resin.
This was repaired by HC + treated with vaseline
(a) Two more (larger) scarabs of this material (qq). Can just be possibly scratched with a knife. Opaque: slight fairly uniform green tint: certainly natural stone:
12
Vulture Head J (Gold with eyes of obsidian)
Cleaned with NH4OH + warm water
Eyes replaced by HC with glue.
Dagger K
Tested small amount of scrapings from corroded spots on surface of blade.
The material of blade was a silvery-grey (like zinc in colour or wrought
iron): it was spotted with corrosion looking like rust.
GR 23/26
The material from corrosion dissolved in HCl is a yellow solution which gave
a blue colour with potassium ferrocyanide + was therefore oxide (or
hydrated oxide) of iron
Blade covered with vaseline by HC.
Bracelet N
Gold + glass inlay.
Cleaned with NH4OH + warm water.
Loose inlay re-fixed by H.C. with glue. Waxed.
Bracelets HH
(a) 1 Gold with barrel-shaped piece of lapis lazuli
(b) 1 " " " " " " poor quality carnelian that is it had
some thin dark bands on one side.
(c) 1 Gold with large sacred eye (Eye was iron.)
(a) + (b) Cleaned with warm water + ammonia.
(c) Had several large patches of dark red corrosion looking like rust. This
gave a yellow solution with HCl which gave a blue coloration with potassium
ferrocyanide
GR 24/26
Cleaned with fine dust + caustic soda (hot)
Washed well + coated with vaseline.
13
Dagger DD
Sheath - gold with delicate inlay on one side.
Gold much discoloured.
Removed discoloration with nitric acid, after trying ammonia + also KCN
without effect. Washed well: treated with ammonia + again washed.
Inlay cleaned with ammonia + warm water + a wooden tooth pick + gold of
inlay with ammonia. Waxed.
Pectoral QQQ
Cleaned with warm water + gold with water and ammonia.
A large patch of silver chloride on lunar disc removed with .880 ammonia
Bracelets X and PP
Cleaned with warm water + gold with warm water + ammonia.
Gold of X poor quality with copper + would not come very bright. Potassium
cyanide darkened it.
Repaired by HC with glue. Waxed.
14
Gold Amulets + Pectorals
T. Soap + water: ammonia: heating in flame of spirit lamp: KCN
KKK. - do -
GG. - do -
Amulets
YYY Lapis lazuli + gold
4B, XXX, 4A
Green felspar + gold
ZZZ Carnelian + gold
Cleaned with ammonia + warm water.
KK Gold
HHH. Bluish green faience turning black in gold frame
FFF. Red Jasper
GGG Green Felspar in gold frame
Cleaned with ammonia + warm water
JJJ Gold
III "
Snake III bis "
Cleaned with ammonia + warm water
15
Uraeus 4Q
Gold with Lapis + glass + stone (translucent) with red cement now decayed.
The stone is fibrous calcite. Body + tail in sections: all plastered with
beeswax to stick it in place on wrappings.
Cleaned with acetone (+CHCl3) + ammonia
Vulture 4R
Gold: plastered with beeswax as above.
Cleaned as above.
MMM also NNN also Z
Large inlaid bird in sections.
Dark blue glass now quite decayed - no colour + much expansion.
Cleaned with ammonia + warm water (after acetone to dissolve fatty matter)
In a number of cases in MMM red glass inlay was covered with a green
deposit + looked exactly like green inlay.
In Z the blue glass in part was in better condition.
Amulets
4L
4K
4J
4I
4I bis
4H
4G
4F
Gold: cleaned with ammonia + warm water
Also C (with tiny crystals of fatty acid) F. G. H. P. C. W. TT and M all
gold + many with white deposit probably of fatty matter: cleaned with
ammonia, heating, nitric acid + warm water.
Also LLL.
16
Coffin 255
White film on jewellery, both on gold + on inlay. (This is distinct from the
cement or the glass of the inlay which in some instances has deteriorated)
No transparent stain when warmed on paper, i.e. not fatty matter.
No Cl
No SO3
Slight pp with AgNO3 soluble in HNO3: no effervescence
noticeable with acid + no alkalinity (but possibly acidity) before adding
AgNO3 or acid, hence not Na2CO3
On one piece of faience inlay (small pendent) a white efflorescence gave a positive test for Cl + a negative test for SO3
Mask 256
Inlay
(a) Blue glass
(b) Whitish, waxy-looking translucent stone.
(b) This scratches glass
Surface undulated like that of some of the glass but undulations not
uniform like those of the glass + the surface was scratched cross-wise,
these scratches appearing to be the marks of working.
GR 25/20
Flail + Crook + Hands 256
Cleaned with ammonia + warm water.
Gold of hands + gold bands of flail + crook much stained reddish brown; this
stain not removed by nitric acid or ammonia
Metal core of flail + crook is silver. (containing copper)
17
Strapping from Outside Mummy
Cleaned from black with acetone + afterwards further cleaned with
NH4OH + warm water.
There was a considerable white efflorescence on the black which proved to be
fatty matter + probably fatty acid. Inlay is lapis lazuli, green felspar,
transparent quartz with a red backing and red + light blue glass.
Replaced loose pieces of inlay + cemented them in with Necol.
Cement is very suggestive of resin or resin plus another material
Gold Girdles
Burned off black: this caused some discoloration owing to copper in gold: treated with strong nitric acid to remove copper discoloration: washed: cleaned with NH4OH + warm water.
Gold Band (From head)
Cleaned with NH4OH + warm water.
Large Vulture from Top of Strapping
Cleaned as for strapping: a little of the red glass had lost or partially lost its colour as well as much of the dark blue glass.
18
Small Bird UUU + Gold Chain
Gold + inlay.
Cleaned with ammonia + warm water
19
Beads (4U + H.H.)
Gold. NH4OH. soap + warm water
Glass. Soap + warm water
TAA i.2.12a.4.20 Not scanned.
21
Gold Band for Forehead ? 4P
A considerable amount of brown resin attached.
Removed resin with acetone: cleaned gold with ammonia + warm water.
Inlaid Gold Apron J
Cleaned with ammonia + warm water: large (+ small) pieces of quartz inlay
with red cement backing
Gold Chains 4D.
4. HC boiled with water.
Treated with HNO3: well washed.
Various 4E.
2 Small Heart-shaped amulets
2 " sitting birds (? doves)
2 " Buckles inlaid
Cleaned with ammonia + warm water.
Bracelets
R.R. Gold + stone (?) Ammonia + warm water. (stone has reticulated pattern)
Not stone, but crocodile or lizard skin
Glows slightly when heated
22
Collars
Two of each
I. Gold with glass inlay in large corrugated strips.
Cleaned with ammonia + warm water
A.A. - Ditto -
Malachite
A green tubular bead of natural stone with green incrustation on surface
which gave a blue colour with ammonia. Probably malachite
Bracelets
WW Stone (Like scarab SS etc) (Hard, but can be just scratched with a
knife, greenish, veined in places
ZZ
Lapis Lazuli
Many tubular beads perished
Rectangular pieces for flexible straps perished